Process instrumentation for a nuclear waste treatment plant

Application Report | Nuclear

  • Safe and sustainable treatment of nuclear liquid waste from Mo-99 radiopharmaceutical production
  • Instrument supply for flow, level, pressure, and temperature measurement
  • Including radioactive waste measurement, hot cell pressure control and chemical dosing
  • Supplies of instruments for nuclear and non-nuclear environments
Background

Australia's Nuclear Science and Technology Organisation (ANSTO) is one of Australia’s largest public research organisations. The institute is widely recognised as an international player in the field of nuclear science and technology.

ANSTO has developed the Synroc® technology which is regarded as global best practice in the safe treatment of complex nuclear waste, including actinide bearing materials, radioiodine, and molten salts from spent fuels. The benefit of this technology is demonstrated in an automated process plant (Synroc Waste Treatment Plant) that the organisation operates near Sydney. The objective of the plant is to treat the liquid by-product of Molybdenum-99 (Mo-99) nuclear medicine production.

Measurement requirements

The liquid waste from Mo-99 production is captured, stored, and characterised in tanks before it is processed within a hot cell by introducing the Synroc formulation. The tailored liquid additive undergoes mixing before it is converted into a granulated powder via a drying process. Subsequently, the powder is then dispensed to a specially designed canister which is then sealed and placed into a Hot Isostatic Press (HIP) where heat and pressure are applied for waste form consolidation. The final solid product is volume-reduced, durable and a disposal-ready waste form.

While the liquid Mo-99 production waste is radioactive, various manufactured components needed to be interrogated for material compatibility within the environment prior to commissioning. One of the main challenges was finding an instrument supplier with experience in radiation sensitive environments.

KROHNE Solution

With a long track record in nuclear applications, offering a wide range of radiation hardened products and components, KROHNE was able to qualify as a preferred instrument supplier.

The instruments in contact with the Mo-99 waste were the first to be specified. This included the POWERFLUX 5300, an electromagnetic flowmeter designed for nuclear environments, which is used for the waste feed and feed control. The most critical installation involved the double remote POWERFLEX 2200 guided radar level transmitter used for waste tank level measurement. To maintain ventilation confinement, various OPTIBAR DP 7060 differential pressure transmitters are used for pressure control and monitoring of the hot cell.

In total, the instrument selections covered various applications incl. flow, level, pressure, and temperature measurement as well as different media – from liquid Mo-99 waste to chemicals and process condensate to clean water. KROHNE supplied among others:

Most instruments have been provided in rugged stainless-steel housing. Critical instruments were proven and demonstrated on a smaller pilot plant to verify the concept before the customer selected the instrument supplied for the Synroc Waste Treatment Plant.

Customer benefits

Selecting KROHNE allowed ANSTO to have a supplier for radiation specific measurements as well as standard applications. Given its vast experience in nuclear applications, KROHNE was able to supply the instruments for a number of unique measurements in contact with nuclear waste.

KROHNE offers various devices designed to operate in nuclear applications inside and outside the nuclear power industry, many of which can also be qualified according to IEEE 323, IEEE 344 and RCC-E standards and designed as per nuclear construction codes such as ASME Section III or RCC-M.

Products used
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OPTIFLUX 4100
Electromagnetic flowmeter for standard applications with abrasive and aggressive liquids
  • Chemically resistant, for liquids (>5 μS/cm) with solid content (≤10%)
  • Up to +180°C / +356°F
  • Flange: DN2.5…1200 / ⅒…48", max. PN40 / ASME Cl 600
  • 4…20 mA, pulse, frequency, status, HART®
OPTIFLUX 5300
Electromagnetic flowmeter for advanced process and master meter applications
  • Highest accuracy (±0.15%), with ceramic tube for aggressive and abrasive liquids (≤70% solid content) up to +180°C / +356°F
  • CT: OIML R117, MI-005 etc.
  • Flange: DN15…300 / ½…12", max. PN40 / ASME Cl 300; Sandwich: DN2.5...100 / ⅒...4"
  • 3 x 4…20 mA, HART®, Modbus, FF, Profibus-PA/DP, PROFINET
OPTIMASS 6400
Coriolis mass flowmeter for advanced process applications
  • High accuracy (±0.05% flat), for cryogenic to HT media (-200…+400°C / -328…+752°F); maintains operation over a wide range of gas fractions and complex flow conditions (EGMTM)
  • SIL 2/3; CT: OIML R117, R137, MI-005, MI-002; API, AGA; hygienic certifications
  • Flange: DN10…300 / ½…12", max. PN 160 / ASME Cl 1500
  • 3 x 4…20 mA, HART®7, Modbus, FF, Profibus-PA/DP, PROFINET, EtherNet/IP™, Bluetooth®
OPTIMASS 7400
Coriolis mass flowmeter for advanced process applications
  • High accuracy (±0.1%), for viscous, aggressive or shear-sensitive media; maintains operation over a wide range of gas fractions and complex flow conditions (EGMTM)
  • CT: OIML R117, MI-005; API; hygienic certifications
  • Flange: DN10…100 / ½…4", max. PN100 / ASME Cl 600; others
  • 3 x 4…20 mA, HART®7, Modbus, FF, Profibus-PA/DP, PROFINET, EtherNet/IP™, Bluetooth®
H250 M40
Variable area flowmeter for liquids and gases
  • Modular design: from mechanical indicator to 4…20 mA/HART®7, FF, Profibus-PA and totalizer
  • Any installation position: vertical, horizontal or in fall pipes
  • Flange: DN15…150 / ½…6"; also NPT, G, hygienic connections, etc.
  • -196…+400°C / -320…+752°F; max. 1000 barg / 14500 psig
OPTIWAVE 7500
Radar (FMCW) level transmitter for liquids in narrow tanks with internal obstructions
  • Continuous, non-contact level measurement in small and narrow tanks with agitators as well as long nozzles
  • 80 GHz radar, flush-mounted Lens antenna
  • Measuring range: 0…100 m / 328 ft
  • -50…+200°C / -58…+392°F; -1…40 barg / -14.5…580 psig
POWERFLEX 2200
Guided radar (TDR) level transmitter for the nuclear industry
  • Continuous measurement of level, distance, volume, mass or dielectric constant
  • Designed and tested for industrial nuclear environments
  • Measuring range: 0.6…40 m / 2…131 ft
  • -50…+150°C / -58…+302°F; -1…100 barg / -14.5…1450 psig
BM26A-1000
Magnetic level indicator for basic liquid applications
  • Cost-effective level measurement; no power supply needed
  • Measuring range: 0.3…5.5 / 1...18 ft (others on request)
  • Density: 700…1200 kg/m / 43.7…74.91 lb/ft3
  • -70…+200°C / -94…+392°F; -1…40 barg / -14.5…580 psig
OPTIBAR PM 5060
Pressure transmitter for process pressure and level applications
  • Rugged design with fully welded metallic diaphragm suited to high pressure ranges and hygienic requirements
  • 100 mbar…1000 bar / 1.45…14500 psi
  • Various threads, flanges, aseptic and other connections
  • 2-wire 4…20 mA/HART®, FF, Profibus-PA, Bluetooth®
OPTIBAR DP 7060
Differential pressure transmitter for flow, level, differential pressure, density and interface measurements
  • High performance DP transmitter with integrated line pressure measurement
  • Measuring range: 30 mbar…16bar / 0.44…232 psi; Line pressure: up to 700 bar / 10,153 psi
  • Reference accuracy of ±0.065%
  • 2-wire, 4…20 mA/HART®, FF, Profibus-PA, Bluetooth®
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